上海口岸进口酒类概况及检测 Napa, California-May 6th,2015

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1 上海口岸进口酒类概况及检测 Napa, California-May 6th,2015
Presented by: HE YUPING, Professor Director , technical center for animal plant and food inspection and quarantine of Shanghai CIQ

2 Agenda 近年来上海口岸进口酒类概况 与酒类检测相关的标准 我们的检测能力
Findings, impact and next steps

3 年进口酒类概况

4 上海口岸进口酒类按国别排行

5 按进口酒分类数重量统计表

6 2013、2014年度进口葡萄酒量排行 法国 $33,440.47 $30,451.24 澳大利亚 $10,582.86 $8,036.05
国别 金额（万美元） 2014 1 法国 $33,440.47 $30,451.24 2 澳大利亚 $10,582.86 $8,036.05 3 智利 $4,454.45 $4,779.91 4 意大利 $3,844.43 $4,247.82 5 美国 $3,620.18 西班牙 $3,541.10 6 $2,902.69 $2,723.61 7 德国 $878.96 $1,007.71 8 阿根廷 $797.11 新西兰 $816.36 9 南非 $778.83 $694.08 10 $774.49 $578.60

7 进口葡萄酒不合格原因分析 标签问题 添加剂使用问题 不符合安全限量要求 半干型标注为干型 用亚硫酸盐代替二氧化硫，用无醇代替脱醇等
无法提供葡萄酒品名的依据 出现“皇家、优质、经典、有机、传统、佳酿、半生态”等引导语 中文品名中的葡萄品种无原文依据 品名中出现年份 品名中有外文字母 橡木桶陈酿无原文依据 采摘年份和葡萄品种无依据 “过量饮酒有害健康”警示语未标 添加剂使用问题 为增加起泡葡萄酒云雾状效果，添加二氧化钛； 检出山梨酸，而标签配料栏中未标识； 不符合安全限量要求 锰、铜、铅超标 二氧化硫超标

8 Agenda 近年来上海口岸进口酒类概况 与酒类检测相关的标准 我们的检测能力 next steps

9 National standards related to the wine 与葡萄酒有关的国家标准
GB National standards for food safety “Fermented alcoholic beverages and their integrated alcoholic beverages” GB 食品安全国家标准“发酵酒及其配制酒” Pb/铅: 0.2 mg/kg Sulfur dioxide/二氧化硫：0.25g/L(for wines) 0.40g/L(for sweet wines and fruit wines) Sorbic acid/山梨酸：0.2g/kg D-isoascorbic acid (erythorbic acid)/D-异抗坏血酸: 0.15g/kg L（+）-tartaric acid/L(+)-酒石酸: 4.0g/L Potassium permanganate(As potassium)/高锰酸钾: 2mg/kg Salmonella/沙门氏菌: 0/25 mL Staphylococcus aureus/金黄色葡萄球菌 : 0/25 mL …

10 National standards related to the wine 与葡萄酒有关的国家标准
The Label of the imported wine should comply with the requirements of "General standard for the labeling of prepackaged foods" (GB ) and “fermented alcoholic beverages and their integrated alcoholic beverages” (GB ). 进口葡萄酒标签应符合“预包装食品标签通则” （GB )和“发酵酒及其配制酒”（GB ）的要求

11 National standards related to the wine 与葡萄酒有关的国家标准
GB the National Standard “Wine” GB 国家标准“葡萄酒” It has taken effect since Jan.1,2008 as compulsory standard. 作为强制标准与2008年1月1日实施。 The standard covers all processes from grape planting, wine production to its transportation. It gives more precise definition of wine and newly adds the sugar content classification. 标准适用于葡萄种植，葡萄酒酿造及运输，并规定了葡萄酒的精确定义和根据总糖含量的分类。 About the industry common concerned issues of vintage wines, varietal wines, and original wines , the standard also gives definition. And the standard regulates the use of wine additives. 关于行业共同关心的年份葡萄酒,品种葡萄酒和产地葡萄酒，标准给出了定义。标准同时对添加剂的使用进行了规定。 Part of this standard defines the equivalent adopted the international organization for OIV regulations(2003 edition). 标准的部分定义等效采用了OIV法规（2003版）

12 “Wine”(GB 15037-2006) ITEM Requirement Degree of Alcohola（20℃）（%vol）
≥7.0 Total sugard（As Glucose）/(g/L) Still wines Dry wineb ≤4.0 Semi-dry winec 4.1~12.0 Semi-sweet wine 12.1~45.0 Sweet wine ≥45.1 Sparkling wines Brut sparkling wine ≤12.0（Tolerance of 3.0） Extra-dry sparkling wine 12.1~17.0（Tolerance of 3.0） Dry sparkling wine 17.1~32.0（Tolerance of 3.0） Semi-dry sparkling wine 32.1~50.0 Sweet sparkling wine ≥50.1 Dry extract/ （g/L） White wine ≥16.0 Rose wine ≥17.0 Red wine ≥18.0 Volatile acids（As acetic acid）/（g/L） ≤1.2 Citric acid dry、semi-dry、semi-sweet wine ≤1.0 ≤2.0

13 “Wine”(GB 15037-2006) ITEM SPECIFICATION Carbon dioxide（20℃）/MPa
Semi-sparkling wine ＜250mL/bottle 0.05~0.29 ≥250mL/bottle 0.05~0.34 Over-sparkling wine ≥0.30 ≥0.35 Iron/（mg/L） ≤8.0 Copper/（mg/L） ≤1.0 Methanol/（mg/L） White or Rose wine ≤250 Red wine ≤400 Benzoic acid or sodium benzoate（As benzoic acid）/（mg/L） ≤50 Sorbic acid and sorbic acid sodium（As Sorbic acid ）/（mg/L） ≤200 Notes： There is no requirement on the total acid which is represented in the measured values(As tartrate, g/L). a. The degree of alcohol marked on the label and the measured value shall not be more than ±1.0% （%vol）. b. When difference between the total sugar and total acid (As tartaric acid) is less than or equal to 2.0 g/L, the total sugar should be up to 9.0 g/L. c. When difference between the total sugar and total acid (As tartaric acid) is less than or equal to 2.0 g/L, the total sugar should be up to 18.0 g/L。 d. The requirement of the total sugar in semi-sparkling wine is the same as in still wine.

14 Norm on Terminology of Imported wines (SB/T 11122-2015) 进口葡萄酒相关术语翻译规范（国内贸易行业标准）
Foreword: This standard collects and sorts related foreign terms of imported wine , and theirs expression, intended to prevent wine imports on the domestic market information transmission of confusion and error, to promote the healthy development of the imported wine market.标准收集、整理了进口葡萄酒相关的外来术语，及其中文表述，旨在防止国内市场上进口葡萄酒信息传递的混乱和错误，促进进口葡萄酒市场的健康发展。 Chapter 2：General Terms基本术语 The basic terminology that may occur on the wine label was included in this standard.收录了在葡萄酒标签上可能出现的葡萄酒基本术语。 Chapter 3： Wine Grape Varieties酿酒葡萄品种 Includes the main grape variety name(not including China), country of origin, variety alias and the fruit color. 收录了世界（不包括中国）主要酿酒葡萄品种名称，原产国，品种别名和果实颜色。 Chapter 4: Principal Countries' Wine Regions and Chateaux主要国家葡萄酒产区及酒庄 4.1 Argentina阿根廷 4.2 Australia澳大利亚 4.3 Chile智利 4.4 France法国 4.5 Germany德国 4.6 Italy意大利 4.7 New Zealand新西兰 4.8 Portugal葡萄牙 4.9 South Africa南非 4.10 Spain西班牙 4.11 USA美国 This standard shall implement on September 1, 2015

15 Agenda 近年来上海口岸进口酒类概况 与酒类检测相关的标准 我们的检测能力 next steps

16 Organization Structure of Technical Center for Animal, Plant and Food Inspection and Quarantine 动植物与食品检验检疫技术中心组织框架 Technical Center 技术中心 Quarantine station for animals and plants 隔离场 Liquor and cosmetics testing center 酒类化妆品检测中心 Genetically modified organism detection and down & feather inspection laboratory 转基因及羽绒室 Plant quarantine and cereal inspection laboratory 植物检疫及粮谷室 Physical and chemical laboratory 理化室 Microbiological laboratory 微生物室 Animal quarantine and toxicology laboratory 动物检疫及毒理室 General Office 办公室

17 Professionals of Liquor and cosmetics testing center 酒类及化妆品检测中心人员
31 dedicated and highly trained professionals work for this center, among whom there are 31名专业技术人员，其中： Professional title 2 senior research scientists, 4 senior professionals 2 intermediate professionals, 2位研究员，4位高级技术人员和2位中级技术人员 Education background 4 doctors, 3 masters 15 bachelors. 学历为：4位博士，3位硕士和15名学士

18 Instrument and Equipment of Liquor and cosmetics testing center 酒类化妆品检测中心设备
To meet the need of ensuring product quality and safety at Shanghai port, the testing center is equipped with many large-scale sophisticated instruments. The total amount of fixed assets has exceeded 11 million USD（614 sets）. 为满足上海口岸进出口酒类安全检测要求，中心配置了614台（套）仪器设备，资产超过1千1百万美元。 HPLC 6 sets; GC 4 sets; IC 1 set; AAS 2 sets; HPLC-MS/MS 2 sets; ICP-MS 1 set; GC-MS 2 sets; Alcolyzer Plus Beer Me 1 set; Thermo Konelab Arena 1 set; Isotope mass spectrometer 1 set

19 Infrastructure of Liquor and cosmetics testing center 酒类化妆品检测中心的面积及业务量
The center occupy an area of 1600 square meters, and the well-arranged and facilitated environment guarantees the quality of lab inspection work. 中心场地面积1600平方米，具有良好的设施和环境，保证检验工作质量满足。 5,469 lots 6,943samples were determined and 27,995 results were reported last year. 去年完成5469批、6943个样品的检测， 出具27995个实验数据。

20 Quality management system of Liquor and cosmetics testing center 酒类及化妆品检测分中心的质量管理体系
Accreditation covering 36 test items on beverage wine and liquor products has been made by China National Accreditation Service for Conformity Assessment (CNAS). 饮料及酒类产品中的36个测试参数通过中国合格评定国家认可委员会（CNAS）的认可 Participate in many domestic and international proficiency tests and collaborative experiments every year and have attained satisfactory results. (FAPAS,CNAS,LGC,TTB) 每年参加许多国内外能力验证和协同试验并取得 满意评价 (如：FAPAS,CNAS,LGC,TTB)） Frequent technical exchanges with delegations and expert teams from foreign authorities such as TTB, CIVB, Pessac, etc. 经常与国外专业机构进行技术交流，如TTB, CIVB, Pessac,等

21 Registration No/认可实验室编号. CNAS L1009
Scope of Accreditation to ISO/IEC 17025:2005 of Liquor and cosmetics testing center 酒类化妆品检测中心认可的检测能力范围 Registration No/认可实验室编号. CNAS L1009 No. Item/Parameter 项目/参数 1 Alcoholicity 酒精度 9 Fusel oil 杂醇油 2 Total sugar 总糖 10 Caffeine 咖啡因 3 Dry extract 干浸出物 11 Acesulfame K 安赛蜜 4 Sulfur dioxide 二氧化硫 12 Total acidity 总酸 5 Volatile acids 挥发酸 13 Formaldehyde 甲醛 6 Iron 铁 14 Ochratoxin A 赭曲霉毒素 7 Copper 铜 15 Citric Acid 柠檬酸 8 Methanol 甲醇  16  Phthalate esters 邻苯二甲酸酯类

22 Ochratoxin A in wine proficiency testing（T1795）
In January 2011, participate in ochratoxin A in wine proficiency testing by FAPAS, the result is satisfactory. The test result of ochratoxin A is 0.95 µg/kg (the median is 1.23 µg/kg) 2011年1月，中心参加英国FAPAS组织的葡萄酒中赭曲霉毒素A的能力验证，测试结果为满意。测定值为0.95 µg/kg (中位值为1.23 µg/kg)

23 Authority as Proficiency Testing Provider 能力验证活动的提供者
2011 Awarded the State Key Testing Laboratory of Alcohol Qualification by AQSIQ 质检总局批准为酒类检测国家重点实验室 2012 Authorized to organize activities of the testing as a proficiency testing provider by Certification and Accreditation Administration（CNCA） 国家认监委授权为能力验证活动提供者组织比对活动 2013 PT of total sugar, sorbic acid, manganese contents in wine(CNCA-13-B14) In April complete validation plan, and sent the invitation to participants A total of 113 laboratories for this PT in China According to the design scheme of the preparation of samples: 2 level and 1 sample disturbance 2013年组织葡萄酒中总糖、山梨酸和锰含量的能力验证活动（CNCA-13-B14） 有113家实验室参加 分发两个测试样品和一个干扰样品

24 Agenda 近年来上海口岸进口酒类概况 与酒类检测相关的标准 我们的检测能力 next steps

25 自身能力建设 做好2015年度国家食品监控计划的监测 完成与葡萄酒检测有关的出入境检验检疫行业标准的起草工作 纳他霉素 富马酸 生物胺
氨基甲酸乙酯 乳糖醇 乙二胺四乙酸 丙酸 4-羟基苯甲酸 邻苯二甲酸酯类 ….. 完成与葡萄酒检测有关的出入境检验检疫行业标准的起草工作 二甘醇 二氧化硫（比色法） 三氯苯甲醚 赭曲霉毒素A 酒香酵母 木塞中酵母、霉菌和细菌

26 国际合作 标签符合性检测工作 参加APEC WRF组织的葡萄酒中成分的环比对实验 承担总局指定的APEC WRF风险控制小组日常工作
葡萄酒中外源糖的同位素比值鉴别 葡萄酒中葡萄品种的分子生物学鉴别 参加APEC WRF组织的葡萄酒中成分的环比对实验 承担总局指定的APEC WRF风险控制小组日常工作

27 Thank you for you attention!